nmRC
Nanoscale and Microscale Research Centre

Confocal Raman Microscope

Logo of the East Midlands Development Agency
 

Originally funded by the East Midlands Development Agency (EMDA), the NMRC hosts a state of the art high speed imaging Raman system; the Horiba LabRAM HR.

Raman spectroscopy and microscopy provides a uniquely sensitive tool for the non-invasive identification of the chemical and physical state of a wide range of samples, rapidly providing quantifiable identification of bulk and surface species.  It is a technique which is used to study the vibrational (and other low-frequency) modes in a system, typically in the range 50 – 4000 cm-1.

Inelastic scattering of laser light off the sample results in a shift of the energy of the scattered photons. This shift gives information about the vibrational modes in the system. Infrared spectroscopy yields similar, but complementary, information.

The LabRAM HR system can be used as a traditional Raman spectrometer to provide vibrational spectra of chemicals, but the most powerful feature of this instrument is its ability to quickly produce confocal images. Four different laser wavelengths are available spanning the UV-Visible-NIR regions giving the user access to an excitation source to match their sample.

The confocal set-up of the microscope gives rise to both clearer images (by reducing contributions from out-of-focus background regions) and the ability to perform depth profiling studies of samples. This instrument is ideally suited for materials and pharmaceutical characterisation, tissue imaging and chemical identification.

The expertise in Raman spectroscopy at Nottingham spans a number of groups across the physical, chemical and biological disciplines.

 NNNCConfocalRaman

 

The Confocal Raman Microscope System 

 

 

RamanStudyExample

Example of study performed with confocal Raman microscope, showing a chemical distribution map (right) and optical image (left).

A. Alkhalil, J. B. Nanubolu, C. J. Roberts, J. W. Aylott, and J. C. Burley, Cryst. Growth Des., 2011, 11, 422–430, 2011, , 422–430

 
 

 

Key Features

  • Confocal depth profiling
  • Four excitation wavelengths available: 325, 532, 660 & 785 nm
  • SWIFT and DuoScan mapping options for fast mapping applications
  • Choice of standard CCD or EM-CCD detectors
  • Variable temperature stage (-196 to 450 ºC)
  • Choice of gratings for standard or high resolution spectroscopy

Further information

For inquiries regarding usage and access please contact Dr. Graham Rance

Additional details about the instrument can be found on the Horiba webpage.

 

Nanoscale and Microscale Research Centre

Cripps South building
University of Nottingham
University Park
Nottingham, NG7 2RD

telephone: +44 (0) 115 748 6340
email: nmrcenquiries@nottingham.ac.uk